Supplements

Ethyl Cinnamate Synthesis

Synthesis of Ethyl Cinnamate
Now to prepare Ethyl Cinnamate, the method is as follows:

Prepare various medicines in advance. Take an appropriate amount of cinnamic acid and place it in a clean reaction vessel. Take anhydrous ethanol and pour it slowly. The amount of ethanol should be sufficient to fully react with cinnamic acid. And add a little concentrated sulfuric acid as a catalyst. The use of concentrated sulfuric acid can promote the speed of the reaction.

Put this mixture on a water bath and heat it slowly. The water bath can be heated evenly to prevent the medicine from being changed due to uneven heating. When heating, it is appropriate to stir with a glass rod from time to time to make the medicine mix evenly and the reaction is fast and complete. When

is reacting, observe it closely. The color of the solution can be seen, or it has changed slightly; or there are micro-bubbles, which are all signs of the reaction going on. After the reaction is completed, remove the fire source and make the reaction liquid slightly cold.

After it is cold, pour it into the separation funnel. Add an appropriate amount of water and shake it. Ethyl cinnamate is insoluble in water and floats on the upper layer, while other substances are either dissolved in water or layered with it. Let stand for a while, until the layering is clear, separate the upper layer of ethyl cinnamate.

Wash it with a saturated sodium carbonate solution, so remove the residual acid. After washing, rinse it with distilled water several times until the wash solution is neutral.

Finally, the washed ethyl cinnamate is placed in a distillation device and distilled to obtain pure ethyl cinnamate. During distillation, control its temperature, so that ethyl cinnamate is slowly steamed out and collected in a clean container.

In this way, ethyl cinnamate can be obtained.